Missy,
Ray have given you a good response suggesting the *OPC command. There is a good example of this on our website...you can find it at the following path:
www.ni.com>>technical support>>advanced search...Check example programs and search for "waiting for operation to complete" and it should be the first example program.
If you are still having trouble using this command, you can insert a sequence structure that with a wait function int he sequence. This should provide enough of a delay for the instrument to setup correctly.
Best Regards,
Chris D
Applications Engineer
National Instruments