Hi,
The first thing you need to do is check the connection in MAX (Measurement and Automation Explorer). Is the instrument detected by MAX when using "scan for instruments"?. If it is, then click on "communicate with instrument". Try a query using a simple command like "*IDN?". If the instrument responds to this query, you canb assume that the GPIB communication is working properly.
What kind of error are you getting?. Is it an instrument error or is the function returning an error?. What are the error messages?. Are you sending the appropriate command?. Change the display of the string control to HEX, to see exactly the characters that are being send.
DiegoF.
National Instruments.